Liquid-Film Assisted Mechanism of Reactive Flash Sintering in Oxide Systems

Liquid Film Capillary Mechanism for Densification of Ceramic Powders during Flash Sintering

Recently, local melting of the particle surfaces confirmed the formation of spark and plasma during spark plasma sintering, which explains the rapid densification mechanism via liquid. A model for rapid densification of flash sintered ceramics by liquid film capillary was presented, where liquid film forms by local melting at the particle contacts, due to Joule heating followed by thermal runaw...

Microwave Assisted Reactive Sintering of Zirconium Oxynitrides

On the Mechanism of Microwave Flash Sintering of Ceramics

The results of a study of ultra-rapid (flash) sintering of oxide ceramic materials under microwave heating with high absorbed power per unit volume of material (10-500 W/cm³) are presented. Ceramic samples of various compositions-Al₂O₃; Y₂O₃; MgAl₂O₄; and Yb(LaO)₂O₃-were sintered using a 24 GHz gyrotron system to a density above 0.98-0.99 of the theoretical value in 0.5-5 min without isothermal...

Resolving the film-formation dilemma with infrared radiation-assisted sintering.

The film formation of an acrylate latex with a glass-transition temperature of 38 °C has been achieved through the use of near-infrared (NIR) radiative heating. A hard, crack-free coating was obtained without the addition of plasticizers. Sintering of acrylate particles was confirmed through measurements using atomic force microscopy. The addition of an NIR-absorbing polymer increased the rate ...

8YSZ sintering by flash sintering method and evaluation of process parameters

Flash sintering as a new sintering method for sintering of ceramic materials has been studied and effect of various parameter such as flash current density, time of flash and contact paste on properties of flash sintered 8YSZ samples has been investigated. Results showed it is possible to achieve high density in shorter time and lower temperature than conventional sintering methods. Samples cou...